# Master Thesis - Synthesis and Characterization of NiAl Layered Double Hydroxides as Precursors for Ni-Based CO₂ Methanation Catalysts

In the field of power-to-gas technologies, the Sabatier reaction is considered a promising approach for converting hydrogen and carbon dioxide into synthetic methane using a catalyst. Nickel supported on alumina is one of the frequently used catalysts. It has been shown that the size and dispersion of the active Ni nanoparticles, as well as their interaction with the support material, are decisive factors for activity. NiAl layered double hydroxides deposited on γ-Al₂O₃ represent promising precursors, as they enable high dispersion of the Ni nanoparticles as well as strong interaction with the support material. To this end, the goal is to elucidate the structure-activity relationship in order to increase the activity and stability of the catalyst. Join us now for this master thesis.

## Your Job

- Synthesis of NiAl LDH as precursors for Ni/γ-Al₂O₃ catalysts
- Optimization of the synthesis and reaction parameters
- Complementary characterization using PXRD, PDF, TGA-MS, DRIFT-FTIR, and N₂ physisorption
- Data analysis using Python, OriginPro …
- Literature review and interpretation of results

The topic offers various focuses and can be adapted based on your interests

## Your Profile

- Currently pursuing a master’s degree in chemistry, Geoscience, chemical engineering, materials science, or a related field
- Responsible and confident in performing chemical laboratory work
- Ability to perform data analysis using the required software
- Ability to work independently and as part of a team
- Interest in and enthusiasm for scientific and experimental work

## Our Benefits for You

We work on the very latest issues that impact our society and are offering you the chance to actively help in shaping the change! We support you in your work with:

- **Meaningful Tasks:** Your thesis deals with a future-oriented, socially relevant topic with direct practical relevance in an international environment
- **Practical relevance:** With us, you will gain valuable practical experience alongside your studies and actively participate in interdisciplinary projects
- **Scientific environment:** You can expect excellent scientific equipment, modern technologies, and qualified support from experienced colleagues
- **Personal responsibility:** You organize your tasks independently—from preparation to implementation
- **Onboarding & teamwork:** You can look forward to working in a dedicated, international, and collegial team. It is important to us that you quickly settle into the team and are given structured training for your tasks. We also support you from the very beginning and make your start easier with our [Welcome Days and Welcome Guide](https://go.fzj.de/welcome)
- **Flexibility:** Flexible working hours make it easier for you to balance work and study
- **Perspective:** If you have the appropriate qualifications and funding is available, the institute offers the opportunity to do your PhD after completing your master's thesis
- **Fair remuneration:** We will pay you a reasonable remuneration for your thesis

In addition to exciting tasks and a collegial working environment, we offer you much more: [https://go.fzj.de/benefits](https://go.fzj.de/benefits)

We welcome applications from people with diverse backgrounds, e.g. in terms of age, gender, disability, sexual orientation / identity, and social, ethnic and religious origin. A diverse and inclusive working environment with equal opportunities in which everyone can realize their potential is important to us.

The following links provide further information on diversity and equal opportunities: [https://go.fzj.de/equality](https://go.fzj.de/equality) and on specific support options: [https://go.fzj.de/womens-job-journey](https://go.fzj.de/womens-job-journey)

**Place of Employment:** Aachen

**Start Date:** To the next possible date

**Application Deadline:** The position will be published until it is successfully filled.

[Application Process](https://go.fzj.de/ApplicationInformation) [FAQ](https://go.fzj.de/FAQ_eng) [Contact form](mailto:karriere@fz-juelich.de?subject=Query%20about%202026M-0481%20Master%20Thesis%20-%20Synthesis%20and%20Characterization%20of%20NiAl%20Layered%20Double%20Hydroxides%20as%20Precursors%20for%20Ni-Based%20CO%E2%82%82%20Methanation%20Catalysts)

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